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Exam 18: The Chemical Literature

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Question 1

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(Note: The next two problems require access to online resources. The answers are available in SciFinder as of July 2000 and not only will vary, but will change as new articles are published. The purpose of these questions is to get students started in online searches; the answers to the questions are not as important as this stated purpose.) -Write down the name of an ingredient listed on a bottle at home. The bottle can be a cleaning item, a medication, a food: whatever you wish. Search for the compound in the Merck Index or in SciFinder. Print the information you find about the compound.

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Question 2

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Use Chemical Abstracts to find all articles that Tarek Sammakia published in 1996.

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Sammakia, Tarek; Hurley, T. Brian. 2-Formyl-4-pyrrolidinopyridine (FPP): A New Catalyst for the Hydroxyl-Directed Methanolysis of Esters. J. Am. Chem. Soc. (1996), 118(37),8967-8968. Sammond, Douglas M.; Sammakia, Tarek. A mild synthesis of substituted furans fromg-hydroxy-a,b-unsaturated ketones. Tetrahedron Lett. (1996), 37(34), 6065-6068. Sammakia, Tarek; Hurley, T. Brian. Hydroxyl directed acyl transfer reactions with2-formyl-4-pyrrolidinopyridine (FPP). Book of Abstracts, 212th ACS National Meeting, Orlando, FL, August 25-29 (1996) Sammakia, Tarek; Hurley, T. Brian; Sammond, Douglas M.; Smith, Randall S.; Sobolov, Susan B.; Oeschger, Thomas R. Dihydroxylation and oxidative cleavage of olefins in the presence of sulfur. Tetrahedron Lett. (1996), 37(26), 4427-4430. Sammakia, Tarek; Hurley, T. Brian; Sammond, Douglas M.; Smith, Randall S.; Sobolov, Susan B.; Oeschger, Thomas R. Dihydroxylation and oxidative cleavage of olefins in the presence of sulfur. Tetrahedron Lett. (1996), 37(26), 4427-4430. Sammakia, Tarek; Latham, Hallie A. On the Mechanism of Oxazoline-Directed Metalations: Evidence for Nitrogen-Directed Reactions. J. Org. Chem. (1996), 61(5), 1629-35.

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Using Lange's Handbook of Chemistry, find the refractive index of each of the following com- pounds. (a) Benzyl alcohol (b) Formamide (c) 3-Pentenoic acid chloride

(Note: The next two problems require access to online resources. The answers are available in SciFinder as of July 2000 and not only will vary, but will change as new articles are published. The purpose of these questions is to get students started in online searches; the answers to the questions are not as important as this stated purpose.) -Use the Merck Index and SciFinder to find out about one of the following topics. Go first to the word in italics and look it up in the Merck Index. Print the record and highlight the CAS registry number. Use this number to help you search SciFinder for the desired information. Print the abstract. Circle the document type; if it is a journal, highlight the journal name. (a) Uses for ferrocene-treated zeolite catalysts (b) The role of benzoic acid in the protection of trembling aspens (c) Find information on the effectiveness of an arginine derivative of ibuprofen in pain man- agement

Using the Merck Index, find the following information. (a) The medical use of a-methyl-p-tyrosine (b) The structure and primary literature reference to tocol (c) What the Wenker ring closure is

Use Chemical Abstracts to find the CAS RN for the following compounds. (a) 1-Cyclohexyl-2-propyn-1-ol (b) Marvinol 2002

Using the Handbook of Chemistry and Physics, find the melting points of the following com- pounds. (a) trans-1,2-Cyclohexanedicarboxylic acid (b) m-Aminophenol (c) 2,5-Dibromofuran

Use Chemical Abstracts to find the name and molecular formula of the compound with the CAS RN [1226-05-7].